Information card for entry 7708855

Structure parameters

• Formula: C28 H42 Cl2 D3 N2 P2 Pd Sn
• Calculated formula: C28 H42 Cl2 D3 N2 P2 Pd Sn
• Title of publication: Stannylenes based on pyrrole-phosphane and dipyrromethane-diphosphane scaffolds: syntheses and behavior as precursors to PSnP pincer palladium(II), palladium(0) and gold(I) complexes.
• Authors of publication: Cabeza, Javier A.; Fernández, Israel; García-Álvarez, Pablo; García-Soriano, Rubén; Laglera-Gándara, Carlos J; Toral, Rubén
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 44
• Pages of publication: 16122 - 16132
• a: 10.7876 ± 0.0004 Å
• b: 12.456 ± 0.0005 Å
• c: 13.68 ± 0.0003 Å
• α: 101.654 ± 0.003°
• β: 108.54 ± 0.003°
• γ: 103.841 ± 0.003°
• Cell volume: 1613.14 ± 0.11 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0315
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.0819
• Weighted residual factors for all reflections included in the refinement: 0.0844
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No