Information card for entry 7708865

Structure parameters

• Formula: C29 H26.6 Cl2.6 F7.4 Ge O5.1 P2 S1.7
• Calculated formula: C29 H26.6 Cl2.6 F7.4 Ge O5.1 P2 S1.7
• Title of publication: Neutral and cationic germanium(IV) fluoride complexes with phosphine coordination – synthesis, spectroscopy and structures
• Authors of publication: King, Rhys; Levason, William; Reid, Gillian
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 11.5994 ± 0.0002 Å
• b: 20.72 ± 0.0004 Å
• c: 14.752 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3545.49 ± 0.1 ų
• Cell temperature: 99.9 ± 0.3 K
• Ambient diffraction temperature: 99.9 ± 0.3 K
• Number of distinct elements: 8
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.0618
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.1001
• Weighted residual factors for all reflections included in the refinement: 0.1046
• Goodness-of-fit parameter for all reflections included in the refinement: 1.163
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No