Information card for entry 7709064

Structure parameters

• Formula: C52 H60 B Cl2 F24 P4 W
• Calculated formula: C52 H60 B Cl2 F24 P4 W
• Title of publication: Dinitrogen-derived (diarylboryl)diazenido Complexes with Differing Coordination to the Thallium Cation
• Authors of publication: Bouammali, Amal; Coffinet, Anaïs; Vendier, Laure; Simonneau, Antoine
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 12.8472 ± 0.0001 Å
• b: 14.4461 ± 0.0001 Å
• c: 19.371 ± 0.0001 Å
• α: 108.898 ± 0.004°
• β: 94.296 ± 0.005°
• γ: 94.608 ± 0.005°
• Cell volume: 3370.85 ± 0.1 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0522
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.1117
• Weighted residual factors for all reflections included in the refinement: 0.1213
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No