Information card for entry 7709295

Structure parameters

• Formula: C101 H55 B2 F48 N2 Pd3
• Calculated formula: C101 H55 B2 F48 N2 Pd3
• Title of publication: Bridging coordination of acenaphthylene to a Pd₃ chain or a Pd₄ sheet cluster.
• Authors of publication: Yamamoto, Koji; Sugawa, Tsuyoshi; Kondo, Mio; Masaoka, Shigeyuki; Murahashi, Tetsuro
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2022
• Journal volume: 51
• Journal issue: 5
• Pages of publication: 1901 - 1906
• a: 14.5164 ± 0.0006 Å
• b: 27.949 ± 0.001 Å
• c: 24.4264 ± 0.001 Å
• α: 90°
• β: 102.955 ± 0.0012°
• γ: 90°
• Cell volume: 9658 ± 0.7 ų
• Cell temperature: 129 K
• Ambient diffraction temperature: 129 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.107
• Residual factor for significantly intense reflections: 0.0763
• Weighted residual factors for significantly intense reflections: 0.1944
• Weighted residual factors for all reflections included in the refinement: 0.2171
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No