Information card for entry 7709922

Structure parameters

• Formula: C56 H128 K N16 P4 Pr
• Calculated formula: C56 H128 K N16 P4 Pr
• Title of publication: Spectroscopic and Electrochemical Characterization of a Pr4+ Imidophosphorane Complex and the Redox Chemistry of Nd3+ and Dy3+ Complexes
• Authors of publication: Rice, Natalie T.; Popov, Ivan A.; Carlson, Rebbeca; Greer, Samuel M.; Boggiano, Andrew C.; Stein, Benjamin William; Bacsa, John; Batista, Enrique R.; Yang, Ping; La Pierre, Henry Storms
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 13.0693 ± 0.0016 Å
• b: 13.9895 ± 0.0017 Å
• c: 23.626 ± 0.003 Å
• α: 75.191 ± 0.004°
• β: 81.487 ± 0.004°
• γ: 65.497 ± 0.004°
• Cell volume: 3795.7 ± 0.8 ų
• Cell temperature: 108.93 K
• Ambient diffraction temperature: 108.93 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0658
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.1224
• Weighted residual factors for all reflections included in the refinement: 0.1271
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No