Information card for entry 7710141

Structure parameters

• Formula: C60 H82 Ge2 N4
• Calculated formula: C60 H82 Ge2 N4
• Title of publication: An α-diiminato germylene family: syntheses, structures, and reactivity towards C-C coupled digermylene and digermylene oxide
• Authors of publication: Liu, Jingjing; Shang, Jianxuan; Wei, Jing; Gao, Fangfang; Hou, Lei; Zeng, FanLong; Li, Anyang; Wang, Wenyuan
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 12.8471 ± 0.0007 Å
• b: 12.1217 ± 0.0007 Å
• c: 18.1718 ± 0.0009 Å
• α: 90°
• β: 104.017 ± 0.002°
• γ: 90°
• Cell volume: 2745.6 ± 0.3 ų
• Cell temperature: 150.15 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1059
• Residual factor for significantly intense reflections: 0.0549
• Weighted residual factors for significantly intense reflections: 0.1265
• Weighted residual factors for all reflections included in the refinement: 0.146
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No