Information card for entry 7710146

Structure parameters

• Formula: C66 H96 Ge2 N4 O
• Calculated formula: C66 H96 Ge2 N4 O
• SMILES: [Ge]1(O[Ge]2[N](=C3C(N2c2c(C(C)C)cccc2C(C)C)=CCCC3)c2c(C(C)C)cccc2C(C)C)N(C2C(=[N]1c1c(C(C)C)cccc1C(C)C)CCCC=2)c1c(C(C)C)cccc1C(C)C.CCCCCC
• Title of publication: An α-diiminato germylene family: syntheses, structures, and reactivity towards C-C coupled digermylene and digermylene oxide
• Authors of publication: Liu, Jingjing; Shang, Jianxuan; Wei, Jing; Gao, Fangfang; Hou, Lei; Zeng, FanLong; Li, Anyang; Wang, Wenyuan
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 12.93 ± 0.005 Å
• b: 15.925 ± 0.008 Å
• c: 17.049 ± 0.008 Å
• α: 73.279 ± 0.018°
• β: 85.825 ± 0.019°
• γ: 71.002 ± 0.018°
• Cell volume: 3178 ± 3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0698
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.107
• Weighted residual factors for all reflections included in the refinement: 0.1187
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 1.34138 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No