Information card for entry 7710924

Structure parameters

• Formula: C98 H182 Al4 Si16
• Calculated formula: C98 H182 Al4 Si16
• Title of publication: Synthesis of bi- and tetradentate poly-Lewis acids by hydroalumination of poly-alkynyl-anthracene derivatives
• Authors of publication: Mitzel, Norbert Werner; Aders, Niklas; Lamm, Jan-Hendrik; Beckmann, Jean Louis; Neumann, Beate; Stammler, Georg
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 15.1482 ± 0.0003 Å
• b: 18.535 ± 0.0003 Å
• c: 23.3981 ± 0.0004 Å
• α: 102.967 ± 0.002°
• β: 103.576 ± 0.002°
• γ: 97.456 ± 0.002°
• Cell volume: 6106.6 ± 0.2 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0687
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1331
• Weighted residual factors for all reflections included in the refinement: 0.1455
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No