Information card for entry 7711480

Structure parameters

• Formula: C229 H324 N16 O20 V4
• Calculated formula: C229 H324 N16 O20 V4
• Title of publication: Non-redox reactivity of V(II) and Fe(II) formamidinates towards CO2 resulting in the formation of novel M(II) carbamates
• Authors of publication: Korona, Krzesimir; Kornowicz, Arkadiusz; Justyniak, Iwona; Terlecki, Michał; Blachowski, Artur; Lewinski, Janusz
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 15.3254 ± 0.0004 Å
• b: 48.4643 ± 0.0015 Å
• c: 15.4889 ± 0.0002 Å
• α: 90°
• β: 90.021 ± 0.002°
• γ: 90°
• Cell volume: 11504.1 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.093
• Residual factor for significantly intense reflections: 0.0723
• Weighted residual factors for significantly intense reflections: 0.1644
• Weighted residual factors for all reflections included in the refinement: 0.1759
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No