Information card for entry 7712217

Structure parameters

• Formula: C105.5 H64 B2 Cl F48 P3 Pb
• Calculated formula: C105.5 H64 B2 Cl F48 P3 Pb
• Title of publication: Synthesis, spectroscopic and structural properties of Sn(II) and Pb(II) triflate complexes with soft phosphine and arsine coordination.
• Authors of publication: Cairns, Kelsey R.; King, Rhys P.; Bannister, Robert D.; Levason, William; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• Journal volume: 52
• Journal issue: 8
• Pages of publication: 2293 - 2308
• a: 12.7607 ± 0.0002 Å
• b: 16.7182 ± 0.0002 Å
• c: 26.6413 ± 0.0003 Å
• α: 78.088 ± 0.001°
• β: 89.049 ± 0.001°
• γ: 69.761 ± 0.001°
• Cell volume: 5208.49 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0383
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0794
• Weighted residual factors for all reflections included in the refinement: 0.0815
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No