Information card for entry 7714120

Structure parameters

• Formula: C32 H84 Ge2 Mn2 O P8
• Calculated formula: C32 H84 Ge2 Mn2 O P8
• Title of publication: Reactions of [(dmpe)₂MnH(C₂H₄)] with hydrogermanes to form germylene, germyl, hydrogermane, and germanide complexes.
• Authors of publication: Price, Jeffrey S.; Vargas-Baca, Ignacio; Emslie, David J. H.; Britten, James F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• a: 26.777 ± 0.018 Å
• b: 9.568 ± 0.003 Å
• c: 9.796 ± 0.005 Å
• α: 90°
• β: 109.1 ± 0.01°
• γ: 90°
• Cell volume: 2372 ± 2 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.1031
• Residual factor for significantly intense reflections: 0.0604
• Weighted residual factors for significantly intense reflections: 0.1473
• Weighted residual factors for all reflections included in the refinement: 0.1562
• Goodness-of-fit parameter for all reflections included in the refinement: 0.95
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No