Information card for entry 7714423

Structure parameters

• Formula: C32 H60 O8 P4 Pd
• Calculated formula: C32 H60 O8 P4 Pd
• Title of publication: Dioxaphosphabicyclooctanes: small caged phosphines from tris(hydroxymethyl)phosphine
• Authors of publication: Nobbs, James David; Tay, Dillon; Yeap, Yoon Hui; Tiong, Yong-Lun; Ye, Suming; Aitipamula, Srinivasulu; Wang, Cun; Cheong, Choon Boon; van Meurs, Martin
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 20.3803 ± 0.0002 Å
• b: 20.3803 ± 0.0002 Å
• c: 9.0334 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3752.08 ± 0.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0439
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.1118
• Weighted residual factors for all reflections included in the refinement: 0.114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No