Information card for entry 7714600

Structure parameters

• Formula: H6 Na6 O58 P4 W14
• Calculated formula: Na6 O78.5 P4 W14
• Title of publication: Heteroelements in polyoxometalates: a study on the influence of different group 15 elements on polyoxometalate formation.
• Authors of publication: Raabe, Jan-Christian; Jameel, Froze; Stein, Matthias; Albert, Jakob; Poller, Maximilian J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 2
• Pages of publication: 454 - 466
• a: 10.8321 ± 0.0002 Å
• b: 12.6641 ± 0.0003 Å
• c: 15.4456 ± 0.0003 Å
• α: 99.1067 ± 0.0016°
• β: 91.2955 ± 0.0016°
• γ: 104.338 ± 0.0018°
• Cell volume: 2022.7 ± 0.08 ų
• Cell temperature: 99.92 ± 0.18 K
• Ambient diffraction temperature: 99.92 ± 0.18 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0296
• Residual factor for significantly intense reflections: 0.0283
• Weighted residual factors for significantly intense reflections: 0.0709
• Weighted residual factors for all reflections included in the refinement: 0.0719
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No