Information card for entry 7714602

Structure parameters

• Formula: As H5.9 Na3.1 O34 W9
• Calculated formula: As K1.35 Na3.15 O47.5 W9
• Title of publication: Heteroelements in polyoxometalates: a study on the influence of different group 15 elements on polyoxometalate formation.
• Authors of publication: Raabe, Jan-Christian; Jameel, Froze; Stein, Matthias; Albert, Jakob; Poller, Maximilian J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 2
• Pages of publication: 454 - 466
• a: 30.0854 ± 0.00009 Å
• b: 30.0854 ± 0.00009 Å
• c: 30.0854 ± 0.00009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 27231.2 ± 0.14 ų
• Cell temperature: 99.95 ± 0.13 K
• Ambient diffraction temperature: 99.95 ± 0.13 K
• Number of distinct elements: 5
• Space group number: 229
• Hermann-Mauguin space group symbol: I m -3 m
• Hall space group symbol: -I 4 2 3
• Residual factor for all reflections: 0.0585
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.0918
• Weighted residual factors for all reflections included in the refinement: 0.107
• Goodness-of-fit parameter for all reflections included in the refinement: 1.12
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No