Information card for entry 7714644

Structure parameters

• Formula: C8 H21 B F4.25 N2
• Calculated formula: C8 H21 B F4.25 N2
• Title of publication: The impact of Lewis acid variation on reactions with di-<i>tert</i>-butyl diazo diesters.
• Authors of publication: Bedi, Vaibhav; Mandal, Dipendu; Hussain, Zahid; Chen, Shi-Ming; Wu, Yile; Qu, Zheng-Wang; Grimme, Stefan; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 2
• Pages of publication: 439 - 443
• a: 8.75 ± 0.002 Å
• b: 8.991 ± 0.003 Å
• c: 15.956 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1255.3 ± 0.6 ų
• Cell temperature: 149.68 K
• Ambient diffraction temperature: 149.68 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0908
• Residual factor for significantly intense reflections: 0.0744
• Weighted residual factors for significantly intense reflections: 0.1971
• Weighted residual factors for all reflections included in the refinement: 0.2216
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0762
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No