Information card for entry 7714672

Structure parameters

• Formula: C59 H88 B2 Cl6 F4 P3 Rh
• Calculated formula: C57 H84 B2 Cl4 F4 P3 Rh
• Title of publication: Diphosphene with a phosphineborane tether and its rhodium complex.
• Authors of publication: Tsurusaki, Akihiro; Takechi, Shingo; Kamikawa, Ken
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 7
• Pages of publication: 2929 - 2936
• a: 10.4512 ± 0.0002 Å
• b: 13.8345 ± 0.0003 Å
• c: 23.1447 ± 0.0004 Å
• α: 97.4885 ± 0.0016°
• β: 96.6648 ± 0.0017°
• γ: 101.852 ± 0.0017°
• Cell volume: 3211.79 ± 0.11 ų
• Cell temperature: 100.02 ± 0.1 K
• Ambient diffraction temperature: 100.02 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0578
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1344
• Weighted residual factors for all reflections included in the refinement: 0.1378
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No