Information card for entry 7715261

Structure parameters

• Formula: C44 H58 N4 O10 V2
• Calculated formula: C44 H58 N4 O10 V2
• Title of publication: Reaction of Ph₂C(X)(CO₂H) (X = OH, NH₂) with [VO(OR)₃] (R = Et, <i>n</i>Pr): structure, magnetic susceptibility and ROP capability.
• Authors of publication: Glenister, Mollie A.; Frese, Josef W. A.; Elsegood, Mark R. J.; Canaj, Angelos B.; Brechin, Euan K.; Redshaw, Carl
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 12
• Pages of publication: 5351 - 5355
• a: 11.7706 ± 0.0006 Å
• b: 12.4661 ± 0.0006 Å
• c: 16.8513 ± 0.0009 Å
• α: 74.0119 ± 0.0008°
• β: 83.5385 ± 0.0008°
• γ: 72.0988 ± 0.0008°
• Cell volume: 2260.9 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0504
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.1024
• Weighted residual factors for all reflections included in the refinement: 0.1091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No