Information card for entry 7715919

Structure parameters

• Formula: C36 H76 N4 O12 Si4
• Calculated formula: C36 H76 N4 O12 Si4
• Title of publication: Stereoselective synthesis of different cyclic tetrasiloxane isomers depending on the superacid catalyst employed.
• Authors of publication: Sonoda, Kanako; Tohnai, Norimitsu; Kaneko, Yoshiro
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 20
• Pages of publication: 8709 - 8715
• a: 9.6119 ± 0.0002 Å
• b: 22.4858 ± 0.0004 Å
• c: 23.6228 ± 0.0004 Å
• α: 90°
• β: 95.304 ± 0.002°
• γ: 90°
• Cell volume: 5083.76 ± 0.16 ų
• Cell temperature: 213 K
• Ambient diffraction temperature: 213 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0557
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1297
• Weighted residual factors for all reflections included in the refinement: 0.1353
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No