Information card for entry 7716309

Structure parameters

• Formula: C27 H40 Cl3 D2 N2 O Sb
• Calculated formula: C27 H40 Cl3 D2 N2 O Sb
• Title of publication: C–H Bond Activation at Antimony(III): Synthesis and Reactivity of Sb(III)-Oxyaryl Species
• Authors of publication: Dunes, Gabriel; Cordier, Marie; Kahlal, Samia; Pollnitz, Alpar; Saillard, Jean-Yves; Silvestru, Cristian; Sarazin, Yann
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 9.7009 ± 0.0008 Å
• b: 17.2182 ± 0.0017 Å
• c: 18.3636 ± 0.0018 Å
• α: 90°
• β: 102.303 ± 0.003°
• γ: 90°
• Cell volume: 2996.9 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0259
• Residual factor for significantly intense reflections: 0.0252
• Weighted residual factors for significantly intense reflections: 0.0579
• Weighted residual factors for all reflections included in the refinement: 0.0581
• Goodness-of-fit parameter for all reflections included in the refinement: 1.157
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No