Information card for entry 7716402

Structure parameters

• Formula: C198 H153 Co4 F72 N39 P12
• Calculated formula: C168 H108 Co4 F42 N24 P7
• Title of publication: Self-assembled Co(II) and Co(III) [M₂L₃] helicates and [M₄L₆] tetrahedra from an unsymmetrical quaterpyridine ligand.
• Authors of publication: Siddique, Rashid G.; McMurtrie, John C.; Clegg, Jack K.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 27
• Pages of publication: 11237 - 11241
• a: 21.0998 ± 0.0004 Å
• b: 21.1425 ± 0.0004 Å
• c: 34.7365 ± 0.0005 Å
• α: 97.032 ± 0.001°
• β: 98.735 ± 0.001°
• γ: 119.772 ± 0.002°
• Cell volume: 12936.4 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1441
• Residual factor for significantly intense reflections: 0.1201
• Weighted residual factors for significantly intense reflections: 0.2963
• Weighted residual factors for all reflections included in the refinement: 0.3123
• Goodness-of-fit parameter for all reflections included in the refinement: 0.978
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No