Information card for entry 7716449

Structure parameters

• Formula: C13 H20 F10 O P Sb
• Calculated formula: C13 H20 F10 O P Sb
• Title of publication: Oxidation-dependent Lewis acidity in chalcogen adducts of Sb/P frustrated Lewis pairs.
• Authors of publication: Krieft, Jonas; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 28
• Pages of publication: 11762 - 11768
• a: 10.6777 ± 0.0002 Å
• b: 11.973 ± 0.0003 Å
• c: 15.3503 ± 0.0003 Å
• α: 87.221 ± 0.002°
• β: 89.312 ± 0.002°
• γ: 77.017 ± 0.002°
• Cell volume: 1910.03 ± 0.07 ų
• Cell temperature: 100 ± 0.11 K
• Ambient diffraction temperature: 100 ± 0.11 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0926
• Weighted residual factors for all reflections included in the refinement: 0.0947
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No