Crystallography Open Database

Information card for entry 7717306

Preview

Coordinates	7717306.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H18 B2 F20 Si
Calculated formula	C44 H18 B2 F20 Si
Title of publication	Reactions of 1,1- and 1,2-bis-boranes with a protic diamine and hydrazine.
Authors of publication	Yeung, Jason; Yeganeh-Salman, Amir; Miao, Linkun; Stephan, Douglas W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	46
Pages of publication	18727 - 18735
a	11.6711 ± 0.0016 Å
b	12.4063 ± 0.0017 Å
c	14.3607 ± 0.0016 Å
α	96.574 ± 0.006°
β	105.057 ± 0.006°
γ	102.001 ± 0.007°
Cell volume	1932.6 ± 0.4 Å³
Cell temperature	149.99 K
Ambient diffraction temperature	149.99 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1211
Residual factor for significantly intense reflections	0.0556
Weighted residual factors for significantly intense reflections	0.105
Weighted residual factors for all reflections included in the refinement	0.1335
Goodness-of-fit parameter for all reflections included in the refinement	1.0494
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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