Information card for entry 7717477

Structure parameters

• Formula: C52 H55 Ag2 B2 Fe N9 P2 S4
• Calculated formula: C52 H55 Ag2 B2 Fe N9 P2 S4
• Title of publication: Stable homogeneous silver(I) catalysts for the highly efficient cycloaddition of azides onto terminal alkynes in water.
• Authors of publication: Kakavand, Meysam; Kozakiewicz-Piekarz, Anna; Neshat, Abdollah
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 46
• Pages of publication: 18458 - 18461
• a: 9.5392 ± 0.0002 Å
• b: 16.116 ± 0.0003 Å
• c: 18.3419 ± 0.0003 Å
• α: 81.786 ± 0.002°
• β: 79.192 ± 0.002°
• γ: 89.248 ± 0.002°
• Cell volume: 2741.06 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0446
• Weighted residual factors for significantly intense reflections: 0.1137
• Weighted residual factors for all reflections included in the refinement: 0.1155
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No