Information card for entry 7717501

Structure parameters

• Formula: C47 H76 Cl3 N3 Ni0.52 O6 P4 Pd1.48
• Calculated formula: C47 H76 Cl3 N3 Ni0.517 O6 P4 Pd1.483
• Title of publication: Simple and easy functionalization of <i>para</i>-hydroxy POCOP-M (M = Ni(II), Pd(II)) pincer complexes: synthesis of multimetallic species.
• Authors of publication: Serrano-García, Juan S; García-Eleno, Marco Antonio; Arenaza-Corona, Antonino; Rufino-Felipe, Ernesto; Valdés, Hugo; Hernandez-Ortega, Simon; Morales-Morales, David
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 2
• Pages of publication: 694 - 699
• a: 12.4109 ± 0.0006 Å
• b: 14.2844 ± 0.0007 Å
• c: 20.6999 ± 0.001 Å
• α: 70.055 ± 0.001°
• β: 85.498 ± 0.001°
• γ: 68.175 ± 0.001°
• Cell volume: 3197.4 ± 0.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2074
• Residual factor for significantly intense reflections: 0.0908
• Weighted residual factors for significantly intense reflections: 0.1997
• Weighted residual factors for all reflections included in the refinement: 0.2552
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No