Information card for entry 7718163

Structure parameters

• Formula: I22 Nb8 O2
• Calculated formula: I22 Nb8 O2
• Title of publication: The family of tetranuclear Nb₄OI_12-<i>x</i> clusters (<i>x</i> = 0, 1, 2): from the molecular Nb₄OI₁₂ cluster to extended chains and layers.
• Authors of publication: Beitlberger, Jan; Martin, Mario; Scheele, Marcus; Schmidt, Patrick; Ströbele, Markus; Meyer, H-Jürgen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 13
• Pages of publication: 5486 - 5493
• a: 10.1217 ± 0.0002 Å
• b: 13.9844 ± 0.0003 Å
• c: 16.3913 ± 0.0003 Å
• α: 88.968 ± 0.002°
• β: 89.093 ± 0.002°
• γ: 85.329 ± 0.002°
• Cell volume: 2311.8 ± 0.08 ų
• Cell temperature: 150.01 ± 0.18 K
• Ambient diffraction temperature: 150.01 ± 0.18 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.021
• Residual factor for significantly intense reflections: 0.0185
• Weighted residual factors for significantly intense reflections: 0.0581
• Weighted residual factors for all reflections included in the refinement: 0.059
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No