Information card for entry 7718509

Structure parameters

• Formula: C52 H104 Cl8 Gd4 O17
• Calculated formula: C52 H104 Cl8 Gd4 O17
• Title of publication: High-yield synthesis of heavy rare earth(III) anhydrous solvates: known, new, and unexpected products.
• Authors of publication: Barbosa, Guilherme A.; Carneiro Neto, José Severiano; Stoeberl, Bruno J.; Wisbeck, Sarita; Giese, Siddhartha O. K.; Yokaichiya, Fabiano; Costa, Daniel da S; Barison, Andersson; Ribeiro, Ronny R.; Piovan, Leandro; Hughes, David L.; Briganti, Matteo; Poneti, Giordano; Nunes, Giovana G.; Santana, Francielli S.; Soares, Jaísa F
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 20
• Pages of publication: 8251 - 8269
• a: 13.2553 ± 0.0011 Å
• b: 10.9651 ± 0.0009 Å
• c: 24.264 ± 0.002 Å
• α: 90°
• β: 97.715 ± 0.004°
• γ: 90°
• Cell volume: 3494.7 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0272
• Residual factor for significantly intense reflections: 0.0222
• Weighted residual factors for significantly intense reflections: 0.0481
• Weighted residual factors for all reflections included in the refinement: 0.0493
• Goodness-of-fit parameter for all reflections included in the refinement: 1.135
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No