Information card for entry 7718581

Structure parameters

• Formula: C46 H76 B Cl2 F6 N O5 Os P2 S2
• Calculated formula: C46 H76 B Cl2 F6 N O5 Os P2 S2
• Title of publication: Syntheses and structures of cationic osmium bis(σ-B-H) borane complexes.
• Authors of publication: Yang, Xiaowen; Tian, Minghui; Wei, Yongliang; Han, Feifei; Wang, Tongdao
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 22
• Pages of publication: 9069 - 9075
• a: 16.85 ± 0.004 Å
• b: 18.96 ± 0.005 Å
• c: 16.99 ± 0.004 Å
• α: 90°
• β: 94.936 ± 0.007°
• γ: 90°
• Cell volume: 5408 ± 2 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 10
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0449
• Residual factor for significantly intense reflections: 0.0364
• Weighted residual factors for significantly intense reflections: 0.0931
• Weighted residual factors for all reflections included in the refinement: 0.0963
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No