Information card for entry 7718584

Structure parameters

• Formula: C64 H48 N4 Pd4 S8
• Calculated formula: C64 H48 N4 Pd4 S8
• Title of publication: A palladium thiolate-SNS complex-catalyst for Mizoroki-Heck cross-coupling.
• Authors of publication: Ataie, Saeed; Khanzadeh, Atousa; Tom Baker, R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 20
• Pages of publication: 8050 - 8054
• a: 11.3905 ± 0.0009 Å
• b: 16.2021 ± 0.0013 Å
• c: 16.8244 ± 0.0013 Å
• α: 100.302 ± 0.002°
• β: 103.645 ± 0.002°
• γ: 102.354 ± 0.002°
• Cell volume: 2860.2 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1345
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.1195
• Weighted residual factors for all reflections included in the refinement: 0.1549
• Goodness-of-fit parameter for all reflections included in the refinement: 0.967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No