Information card for entry 7718620

Structure parameters

• Formula: C9 H13 Cs3.5 N9 Na1.5 O6.5 Se4 W3
• Calculated formula: C9 Cs3.48 N9 Na1.5 O8.02 Se4 W3
• Title of publication: Tungsten oxide as a universal source for the synthesis of complexes with different nuclearities in WO₃/chalcogen/NaCN systems.
• Authors of publication: Yarovoy, Spartak S.; Mirzaeva, Irina V.; Sukhikh, Taisiya S.; Mironov, Yuri V.; Yanshole, Vadim; Brylev, Konstantin A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 21
• Pages of publication: 8644 - 8657
• a: 11.7075 ± 0.0005 Å
• b: 11.7075 ± 0.0005 Å
• c: 44.409 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5271.4 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.0691
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.1687
• Weighted residual factors for all reflections included in the refinement: 0.186
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No