Information card for entry 7718694

Structure parameters

• Formula: C14 H9 Cl0.5 Na5 O177 Pr4 Sb4 W42
• Calculated formula: C14 H9 Cl0.5 Na5 O177 Pr4 Sb4 W42
• Title of publication: A tetranuclear Pr-W heterometal cluster-imbedded antimotungstate for the catalytic synthesis of benzimidazoles.
• Authors of publication: Zheng, Zhijian; Jiang, Song; Chen, Xuejiao; Liu, Haoqi; Liu, Yufeng; Dong, Yayu; Sun, Xiaopeng; Yang, Guoping
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 23
• Pages of publication: 9291 - 9295
• a: 13.5636 ± 0.0008 Å
• b: 19.4915 ± 0.0011 Å
• c: 48.477 ± 0.003 Å
• α: 85.183 ± 0.002°
• β: 85.802 ± 0.002°
• γ: 69.864 ± 0.002°
• Cell volume: 11976.8 ± 1.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1099
• Residual factor for significantly intense reflections: 0.1018
• Weighted residual factors for significantly intense reflections: 0.2731
• Weighted residual factors for all reflections included in the refinement: 0.2823
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No