Information card for entry 7718994

Structure parameters

• Formula: C65 H63 N2 P3 Ru Zn
• Calculated formula: C65 H63 N2 P3 Ru Zn
• Title of publication: Attempted syntheses of ZnPhos-ruthenium complexes (ZnPhos = bis(2-diphenylphosphinophenyl)zinc).
• Authors of publication: Walsh, Amber M.; Lewis, Ludovic J.; Lowe, John P.; Mahon, Mary F.; Whittlesey, Michael K.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 29
• Pages of publication: 11371 - 11381
• a: 12.2341 ± 0.0002 Å
• b: 40.5533 ± 0.0005 Å
• c: 11.3285 ± 0.0001 Å
• α: 90°
• β: 102.525 ± 0.001°
• γ: 90°
• Cell volume: 5486.69 ± 0.12 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0346
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0629
• Weighted residual factors for all reflections included in the refinement: 0.066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No