Information card for entry 7719053

Structure parameters

• Formula: C34 H30 Cl2 N P
• Calculated formula: C34 H30 Cl2 N P
• Title of publication: The investigation of the steric hindrance of anilines by means of reactions with PCl₃ and BCl₃.
• Authors of publication: Němec, Vlastimil; Samsonov, Maksim A.; Růžičková, Zdeňka; Vrána, Jan; Růžička, Aleš
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 31
• Pages of publication: 11845 - 11856
• a: 10.3995 ± 0.0007 Å
• b: 11.8978 ± 0.0007 Å
• c: 12.6174 ± 0.0007 Å
• α: 81.018 ± 0.003°
• β: 73.125 ± 0.003°
• γ: 72.945 ± 0.004°
• Cell volume: 1423.94 ± 0.15 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0446
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0992
• Weighted residual factors for all reflections included in the refinement: 0.105
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No