Information card for entry 7719087

Structure parameters

• Formula: C31 H31 Ag Br N O P
• Calculated formula: C31 H31 Ag Br N O P
• Title of publication: Sterically hindered P,N-type amidophosphines {{(<i>o</i>-PPh₂)C₆H₄}C(O)NH(R)}: synthesis, transition metal chemistry, and catalytic activity in stereoselective Heck coupling of aryl chlorides.
• Authors of publication: Sabharwal, Gazal; Dwivedi, Khilesh C.; Balakrishna, Maravanji S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 30
• Pages of publication: 11551 - 11562
• a: 9.039 ± 0.002 Å
• b: 19.088 ± 0.005 Å
• c: 16.471 ± 0.004 Å
• α: 90°
• β: 101.545 ± 0.006°
• γ: 90°
• Cell volume: 2784.4 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0361
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.077
• Weighted residual factors for all reflections included in the refinement: 0.0808
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No