Information card for entry 7719091

Structure parameters

• Formula: C52 H42 Cu I N O P
• Calculated formula: C52 H42 Cu I N O P
• Title of publication: Sterically hindered P,N-type amidophosphines {{(<i>o</i>-PPh₂)C₆H₄}C(O)NH(R)}: synthesis, transition metal chemistry, and catalytic activity in stereoselective Heck coupling of aryl chlorides.
• Authors of publication: Sabharwal, Gazal; Dwivedi, Khilesh C.; Balakrishna, Maravanji S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 30
• Pages of publication: 11551 - 11562
• a: 38.197 ± 0.006 Å
• b: 8.4181 ± 0.0018 Å
• c: 26.215 ± 0.005 Å
• α: 90°
• β: 90.74 ± 0.006°
• γ: 90°
• Cell volume: 8429 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0446
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.08
• Weighted residual factors for all reflections included in the refinement: 0.0862
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No