Information card for entry 7719109

Structure parameters

• Formula: C40 H54 B10 F18 N P
• Calculated formula: C40 H54 B10 F18 N P
• Title of publication: Synthesis and characterization of <i>closo</i>-decahydrido-decaborate-phosphine mediated by palladium(0) complexes.
• Authors of publication: Haidar Ahmad, Zainab; Cordier, Marie; Naoufal, Daoud; Darcel, Christophe
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 32
• Pages of publication: 12135 - 12140
• a: 20.055 ± 0.003 Å
• b: 21.695 ± 0.003 Å
• c: 23.026 ± 0.003 Å
• α: 86.775 ± 0.004°
• β: 89.378 ± 0.004°
• γ: 89.376 ± 0.004°
• Cell volume: 10001 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1524
• Residual factor for significantly intense reflections: 0.1122
• Weighted residual factors for significantly intense reflections: 0.2606
• Weighted residual factors for all reflections included in the refinement: 0.2862
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No