Information card for entry 7719111

Structure parameters

• Formula: C37 H66 B10 N P
• Calculated formula: C37 H66 B10 N P
• Title of publication: Synthesis and characterization of <i>closo</i>-decahydrido-decaborate-phosphine mediated by palladium(0) complexes.
• Authors of publication: Haidar Ahmad, Zainab; Cordier, Marie; Naoufal, Daoud; Darcel, Christophe
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 32
• Pages of publication: 12135 - 12140
• a: 9.756 ± 0.0011 Å
• b: 18.4904 ± 0.0016 Å
• c: 23.185 ± 0.002 Å
• α: 90°
• β: 100.264 ± 0.004°
• γ: 90°
• Cell volume: 4115.5 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1194
• Residual factor for significantly intense reflections: 0.0865
• Weighted residual factors for significantly intense reflections: 0.2067
• Weighted residual factors for all reflections included in the refinement: 0.2314
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No