Information card for entry 7719198

Structure parameters

• Formula: C58 H72 N8 Ni4 O19
• Calculated formula: C58 H58 N8 Ni4 O19
• Title of publication: Coordination clusters with a [Ni₄O₄] core as catalysts for α-alkylation of ketones with benzyl alcohols.
• Authors of publication: Kajal, ?; Kumar, Manish; Nayek, Hari Pada
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 35
• Pages of publication: 13326 - 13336
• a: 13.7466 ± 0.0007 Å
• b: 15.1921 ± 0.0008 Å
• c: 18.7516 ± 0.001 Å
• α: 101.961 ± 0.004°
• β: 110.604 ± 0.005°
• γ: 104.385 ± 0.004°
• Cell volume: 3357.9 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1101
• Residual factor for significantly intense reflections: 0.0763
• Weighted residual factors for significantly intense reflections: 0.2378
• Weighted residual factors for all reflections included in the refinement: 0.2678
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No