Information card for entry 7719477

Structure parameters

• Formula: C29.5 H37 Cl3 N3 O Rh
• Calculated formula: C28 H34 N3 O Rh
• Title of publication: Rhodium(I) complexes with proton-responsive anionic tethered N-heterocyclic carbene ligands: synthesis and application in alkyne dimerization.
• Authors of publication: Karataş, Mert Olgun; Hinojosa, Diego R.; Passarelli, Vincenzo; Oro, Luis A.; Pérez-Torrente, Jesús J; Castarlenas, Ricardo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 40
• Pages of publication: 15306 - 15319
• a: 9.855 ± 0.0015 Å
• b: 10.5806 ± 0.0016 Å
• c: 28.689 ± 0.004 Å
• α: 90°
• β: 96.195 ± 0.002°
• γ: 90°
• Cell volume: 2974 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0605
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.1015
• Weighted residual factors for all reflections included in the refinement: 0.1061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.125
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No