Information card for entry 7719690

Structure parameters

• Formula: C39 H31 Cl5 N2 O2 P Re
• Calculated formula: C38 H29 Cl3 N2 O2 P Re
• Title of publication: Dual deoxygenation in an α-ketoimine chelated rhenium(III) complex: structural and mechanistic interpretations.
• Authors of publication: Sinha, Ankita; Banerjee, Suparna; Sen, Suphal; Ghosh, Aniruddha; Dey, Arindam; Naskar, Tilak; Singh, Tejender; Gangopadhyay, Jaydip
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 46
• Pages of publication: 17137 - 17150
• a: 11.0316 ± 0.0009 Å
• b: 13.7471 ± 0.0012 Å
• c: 15.4809 ± 0.0013 Å
• α: 75.994 ± 0.002°
• β: 76.868 ± 0.002°
• γ: 80.556 ± 0.002°
• Cell volume: 2203.5 ± 0.3 ų
• Cell temperature: 297 K
• Ambient diffraction temperature: 297 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0446
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0765
• Weighted residual factors for all reflections included in the refinement: 0.0831
• Goodness-of-fit parameter for all reflections included in the refinement: 1.16
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No