Information card for entry 7719775

Structure parameters

• Formula: C93.53 H87.83 Au B Cl0.83 F24.38 N0.97 P
• Calculated formula: C93.52 H87.79 Au B Cl0.828 F24.382 N0.97 P
• Title of publication: Single-crystal to single-crystal synthesis of a gold(I)-ammonia complex and H/D exchange <i>in crystallo</i> with D₂O.
• Authors of publication: Johnson, Chloe L.; Altus, Kristof M.; Navarro, Miquel; Campos, Jesús; Duckett, Simon B.; Weller, Andrew S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 45
• Pages of publication: 16673 - 16676
• a: 14.8156 ± 0.0001 Å
• b: 33.8381 ± 0.0003 Å
• c: 19.0978 ± 0.0002 Å
• α: 90°
• β: 108.338 ± 0.001°
• γ: 90°
• Cell volume: 9088.12 ± 0.15 ų
• Cell temperature: 110.01 ± 0.1 K
• Ambient diffraction temperature: 110.15 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1093
• Residual factor for significantly intense reflections: 0.095
• Weighted residual factors for significantly intense reflections: 0.1846
• Weighted residual factors for all reflections included in the refinement: 0.193
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No