Information card for entry 7719915

Structure parameters

• Formula: C334 H321 Cl6 Cu44 N19 O24 P24
• Calculated formula: C334 H321 Cl6 Cu44 N19 O24 P24
• Title of publication: High-nuclearity Cu hydride nanoclusters of Cu₂₂H₁₉ and Cu₂₀H₁₃ consolidated by an N-containing triphosphine ligand: synthesis, characterization and catalysis.
• Authors of publication: Ma, Meng-Xia; Zhou, Yi-Wu; Gui, Zi-Jian; Huang, Ting-Hong; Ni, Qing-Ling; Li, Shi-Ming; Gui, Liu-Cheng; Wang, Xiu-Jian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• a: 23.1531 ± 0.0002 Å
• b: 29.1303 ± 0.0003 Å
• c: 36.0582 ± 0.0003 Å
• α: 74.06 ± 0.001°
• β: 74.549 ± 0.001°
• γ: 81.862 ± 0.001°
• Cell volume: 22478 ± 0.4 ų
• Cell temperature: 100 ± 0.11 K
• Ambient diffraction temperature: 100 ± 0.11 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0935
• Residual factor for significantly intense reflections: 0.0817
• Weighted residual factors for significantly intense reflections: 0.2416
• Weighted residual factors for all reflections included in the refinement: 0.251
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No