Information card for entry 7720041

Structure parameters

• Formula: C54 H77 Li2 N
• Calculated formula: C54 H77 Li2 N
• Title of publication: Electrophilic lithium carbazolide as an efficient trap for organolithium species: complexes containing monomeric <i>n</i>-BuLi, <i>t</i>-BuLi and Me₃SiCH₂Li units.
• Authors of publication: Bogachev, Mikhail A.; Selikhov, Alexander N.; Cherkasov, Anton V.; Aysin, Rinat R.; Trifonov, Alexander A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2026
• Journal volume: 55
• Journal issue: 6
• Pages of publication: 2452 - 2464
• a: 22.7861 ± 0.0005 Å
• b: 19.6508 ± 0.0003 Å
• c: 23.5221 ± 0.0005 Å
• α: 90°
• β: 113.266 ± 0.002°
• γ: 90°
• Cell volume: 9675.9 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1267
• Residual factor for significantly intense reflections: 0.0765
• Weighted residual factors for significantly intense reflections: 0.186
• Weighted residual factors for all reflections included in the refinement: 0.2214
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No