Crystallography Open Database

Information card for entry 7720355

7720354 << 7720355 >> 7720356

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Coordinates	7720355.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H32 B Cl3 Mo N2 P
Calculated formula	C34 H32 B Cl3 Mo N2 P
Title of publication	Molybdenum(VI) borano-imido complexes and their application as Lewis acid catalysts in homocoupling of diazo compounds
Authors of publication	Škoch, Karel; Buziková, Michaela; Jakubczyk, Michal; Pattanamcheril Anilkumar, Krishna; Demel, Jan; Litecká, Miroslava
Journal of publication	Dalton Transactions
Year of publication	2026
a	9.72725 ± 0.0001 Å
b	10.29523 ± 0.00009 Å
c	18.78662 ± 0.0001 Å
α	91.7045 ± 0.0005°
β	97.5172 ± 0.0007°
γ	118.007 ± 0.001°
Cell volume	1637.81 ± 0.03 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0276
Residual factor for significantly intense reflections	0.027
Weighted residual factors for significantly intense reflections	0.0734
Weighted residual factors for all reflections included in the refinement	0.0738
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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