Information card for entry 7720443

Structure parameters

• Formula: C39 H67 Ca N3 Si2
• Calculated formula: C39 H67 Ca N3 Si2
• Title of publication: Synthesis of heteroleptic calcium amide complexes <i>via</i> manipulation of the Schlenk equilibrium.
• Authors of publication: de Vere-Tucker, Matthew; Slawin, Alexandra M. Z.; Cordes, David B.; Stasch, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2026
• Journal volume: 55
• Journal issue: 4
• Pages of publication: 1708 - 1715
• a: 11.921 ± 0.0009 Å
• b: 29.295 ± 0.002 Å
• c: 13.3529 ± 0.0009 Å
• α: 90°
• β: 113.11 ± 0.0017°
• γ: 90°
• Cell volume: 4289 ± 0.5 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.047
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.1113
• Weighted residual factors for all reflections included in the refinement: 0.1177
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No