Information card for entry 7720924

Structure parameters

• Formula: C24 H48 Dy2 I4 N2 O12
• Calculated formula: C24 H48 Dy2 I4 N2 O12
• Title of publication: Synthesis of hydroxo-bridged Dy(III) dimers supported by crown ethers through C-H activation and oxygen-atom transfer of Me3NO
• Authors of publication: Gu, Ziyi; Li, Jun; Zhang, Xuan; Li, Yangjuan; Gong, Yu
• Journal of publication: Dalton Transactions
• Year of publication: 2026
• a: 8.6671 ± 0.0004 Å
• b: 20.8623 ± 0.0009 Å
• c: 11.8901 ± 0.0005 Å
• α: 90°
• β: 109.78 ± 0.005°
• γ: 90°
• Cell volume: 2023.07 ± 0.17 ų
• Cell temperature: 180 ± 0.1 K
• Ambient diffraction temperature: 180 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0472
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0876
• Weighted residual factors for all reflections included in the refinement: 0.1017
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No