Crystallography Open Database

Information card for entry 7720928

7720927 << 7720928 >> 7720929

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Coordinates	7720928.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H43 Dy I3 N3 O9
Calculated formula	C22 H43 Dy I3 N3 O9
Title of publication	Synthesis of hydroxo-bridged Dy(III) dimers supported by crown ethers through C-H activation and oxygen-atom transfer of Me3NO
Authors of publication	Gu, Ziyi; Li, Jun; Zhang, Xuan; Li, Yangjuan; Gong, Yu
Journal of publication	Dalton Transactions
Year of publication	2026
a	26.437 ± 0.0007 Å
b	8.6873 ± 0.0003 Å
c	30.4259 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	6987.8 ± 0.4 Å³
Cell temperature	179.99 ± 0.1 K
Ambient diffraction temperature	179.99 ± 0.1 K
Number of distinct elements	6
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0447
Residual factor for significantly intense reflections	0.0311
Weighted residual factors for significantly intense reflections	0.057
Weighted residual factors for all reflections included in the refinement	0.0607
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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