Crystallography Open Database

Information card for entry 7720940

7720939 << 7720940 >> 7720941

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Coordinates	7720940.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H75 Mo N6 O3 Si3 W0
Calculated formula	C66 H75 Mo N6 O3 Si3
Title of publication	N-Heterocyclic Silylene Complexes of Group VI Transition Metal Carbonyls
Authors of publication	Glok, Eduard; Schanbacher, Moritz; Luz, Christian; Radius, Udo
Journal of publication	Dalton Transactions
Year of publication	2026
a	12.0795 ± 0.0001 Å
b	12.3043 ± 0.0001 Å
c	22.1867 ± 0.0002 Å
α	73.957 ± 0.001°
β	88.048 ± 0.001°
γ	77.922 ± 0.001°
Cell volume	3098.03 ± 0.05 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	99.99 ± 0.1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0259
Residual factor for significantly intense reflections	0.0247
Weighted residual factors for significantly intense reflections	0.0643
Weighted residual factors for all reflections included in the refinement	0.0649
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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