Information card for entry 7720940

Structure parameters

• Formula: C66 H75 Mo N6 O3 Si3 W0
• Calculated formula: C66 H75 Mo N6 O3 Si3
• Title of publication: <i>N</i>-heterocyclic silylene complexes of group VI transition metal carbonyls.
• Authors of publication: Glok, Eduard; Schanbacher, Moritz; Luz, Christian; Radius, Udo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2026
• Journal volume: 55
• Journal issue: 21
• Pages of publication: 8323 - 8331
• a: 12.0795 ± 0.0001 Å
• b: 12.3043 ± 0.0001 Å
• c: 22.1867 ± 0.0002 Å
• α: 73.957 ± 0.001°
• β: 88.048 ± 0.001°
• γ: 77.922 ± 0.001°
• Cell volume: 3098.03 ± 0.05 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 99.99 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0259
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0643
• Weighted residual factors for all reflections included in the refinement: 0.0649
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No