Information card for entry 7721016

Structure parameters

• Formula: C52 H65 Al F4 K N O7
• Calculated formula: C52 H65 Al F4 K N O7
• Title of publication: Synthesis of Lewis acid-base adducts between trimesityltrieles and potassium cyanate and its heavier homologues
• Authors of publication: Dollberg, Kevin; Lochte, Mark; Weiß, Pauline; Nitzsche, Joel; Mészáros, Katalin; von Hänisch, Carsten; Tambornino, Frank
• Journal of publication: Dalton Transactions
• Year of publication: 2026
• a: 14.3321 ± 0.0002 Å
• b: 24.464 ± 0.0005 Å
• c: 29.155 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10222.3 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1028
• Residual factor for significantly intense reflections: 0.0801
• Weighted residual factors for significantly intense reflections: 0.207
• Weighted residual factors for all reflections included in the refinement: 0.2228
• Goodness-of-fit parameter for all reflections included in the refinement: 0.978
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54186 Å
• Diffraction radiation type: CuKα
• Diffraction radiation X-ray symbol: K-L~2,3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No