Crystallography Open Database

Information card for entry 8000044

Preview

Coordinates	8000044.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C102 H86 Ag4 O9 P4 S4
Calculated formula	C102.35 H80 Ag4 O9.55 P4 S4
Title of publication	Synthesis and Structure of a Molecular Metal Propeller with Three Leaves, a Tetranuclear Silver(I) Cluster Formed by 2-Mercaptobenzoate and Triphenylphosphine Ligands
Authors of publication	Ryusuke Noguchi; Akihiro Hara; Akiyoshi Sugie; Sawako Tanabe; Kenji Nomiya
Journal of publication	Chemistry Letters
Year of publication	2005
Journal volume	34
Journal issue	4
Pages of publication	578
a	37.626 ± 0.008 Å
b	29.464 ± 0.006 Å
c	25.4 ± 0.005 Å
α	90°
β	132.258 ± 0.003°
γ	90°
Cell volume	20841 ± 8 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0893
Residual factor for significantly intense reflections	0.0629
Weighted residual factors for significantly intense reflections	0.2177
Weighted residual factors for all reflections included in the refinement	0.2362
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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