Information card for entry 8101190

Structure parameters

• Common name: [K([2.2.2]crypt)] salt of Nonastannide(3-), 0.5 ethylenediamine solvate
• Formula: C55 H112 K3 N7 O18 Sn9
• Calculated formula: C55 H112 K3 N7 O18 Sn9
• Title of publication: Crystal structure of tris[2.2.2]crypt-kalium nonastannide(3‒)— ethylenediamine (2/1), C~55~H~112~K~3~N~7~O~18~Sn~9~
• Authors of publication: Fässler, Thomas F.; Hoffmann, Rudolf
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2000
• Journal volume: 215
• Journal issue: 1
• Pages of publication: 139 - 142
• a: 14.896 ± 0.003 Å
• b: 16.279 ± 0.003 Å
• c: 20.375 ± 0.004 Å
• α: 92.74 ± 0.03°
• β: 96.51 ± 0.03°
• γ: 111.81 ± 0.03°
• Cell volume: 4535.8 ± 1.6 ų
• Cell temperature: 243 ± 2 K
• Ambient diffraction temperature: 243 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0622
• Weighted residual factors for significantly intense reflections: 0.1802
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No